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Evaporation Tables & Crucible Recommendations

EVAPORATION
MATERIAL
TEMPERATURE (șC)
@ VAP. PRESSURE
EVAPORATION TECHNIQUES REMARKS
n = Index
of Refraction
10-8
TORR
10-6
TORR
10-4
TORR
ELECTRON
BEAM
CRUCIBLE COIL BOAT
Glass,
Schott 8329
Excel. Evaporable alkali glass. Melt in air before evaporating. n = 1.47
Gold (Au) 807 947 1132 Excel. Al2O3 BN
Vit. Carbon
W W, Mo
Coated
Al2O3
Films soft, not very adherent.
Hatnium (Hf) 2160 2250 3090 Good
Hafnium
Carbide (HfC)
-2600S
Hafnium
Oxide (HfO2)
-2500 Fair W Film HfO n = 2.0 @ .5” App. Opt. Apr. 1977
Holmium (Ho) 650S 770S 950S Good W W Ta
Holmium
Fluoride (HoF3)
-800 Quartz
Holmium
Oxide (Ho2O3)
Ir Loses oxygen.
Inconel
(Ni/Cr/Fe)
Good W W Use fine wire pre-wrapped on W. Low rate req'd. for smooth films.
Indium (In) 487 597 742 Excel.;
Mo Liner
req'd
Graphite
Al2O3
W W Mo Wets W and Cu; use Mo liner in guns.
Indium
Antimonide (InSb)
500 -400 W Toxic, Decomposes; sputtering preferred; or co-evaporate from 2 sources; flash. n = 4.3 @ 1”
Indium
Arsenide (InAs)
780 870 970 W Toxic, Decomposes; sputtering preferred; or co-evaporate from 2 sources; flash. n = 4.5 @ 1”
Indium
Oxide (In2O3)
-1200S Good Al2O3 W Pt Film In2O; transparent conductor. JVST 12, 99 (1975)
Indium
Phosphide (InP)
630 730 Graphite W Ta Deposits P rich. Flash evaporate.
Indium
Selenide (In2Se3)
Sputtering preferred; or co-evaporate from 2 sources; flash.
Indium
Sesquisulphide (In2S3)
850S Graphite Film In2S
Indium
Sulphide (In2S)
650 Graphite
Indium
Telluride (In2Te3)
Sputtering preferred; or co-evaporate from 2 sources; flash.
Iridium (Ir) 1850 2080 2380 Fair ThO2
Iron (Fe) 858 998 1180 Excel. Al2O3
BeO
W W Attacks W. Films hard, smooth. Use gentle preheat to outgas.
Iron
Bromide (FeBr2)
561 Fe
Iron
Chloride (FeCl2)
300S Fe
Iron
Iodide (FeI2)
400 Fe
Iron
Oxide (FeO)
Poor Decomposes; sputtering preferred.
Iron
Oxide (Fe2O3)
Good W Disproportionates to Fe3O4 at 1530șC, n = 3.0
Iron
Sulphide (FeS)
Al2O3 Decomposes.
Kanthal (FeCrAl) -1150 W W JVST 7, 739 (1980)
Lanthanum (La) 990 1212 1388 Excel. Al2O3 W Ta Films will burn in air if scraped.
Lanthanum
Boride (LaB6)
Good
Lanthanum
Bromide (LaBr3)
n = 1.94 Hygroscopic.
Lanthanum
Fluoride (LaF3)
900S Good Ta Mo No decomposition. n = 1.59 @ .55”
Lanthanum
Oxide (La2O3)
1400 Good W Ta Loses oxygen. n = 1.9 @ .5”
Lead (Pb) 342 427 497 Excel. Al2O3
Quartz
W W Mo Toxic. Carefully controlled rates req'd. for superconductors.
Lead
Bromide (PbBr2)
-300
Lead
Chloride (PbCl2)
-325 Al2O3 Pt Little decomposition. n = 2.2
Lead
Fluoride (PbF2)
-400 BeO W Pt,
Mo
Toxic. n = 1.75 @ .3”

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Key:
S = Sublime
D = Decomposes
Excel. = Excellent



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